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Reference 600™

The Reference 600 has been replaced with the Reference 600+

System Highlights

Overview

The Reference 600 is a high-performance, research-grade potentiostat/galvanostat/ZRA designed for fast, low-current measurements.  It does well for a variety of applications such as physical electrochemistry (especially at microelectrodes), fast cyclic voltammetry, electrochemical corrosion, electrochemical noise measurements, paints and coatings, and sensors.  

It has a number of auxiliary input and outputs designed to help you interface or control ancillary equipment such as a rotating disc electrode. It also has a thermocouple for temperature measurements. 

Electrochemical Impedance Spectroscopy

The Reference 600 comes fully equipped to perform electrochemical impedance spectroscopy.  The Accuracy Contour Plot shown below provides a detailed look at the performance you can expect from your instrument in real-world situations. The results include the cell cable.

Reference 600 Potentiostat Accuracy Contour Plot

 

Options

  • Extended Cable Lengths
    • Extended length cell cables (1.5 m, 3 m, 10 m) are also available for your convenience.

More details

Below are additional details regarding the capabilities of the Reference 600 potentiostat. Each bullet point contains a list of the type of techniques available for the instrument to run.

  • Physical Electrochemistry  - Techniques such as cyclic voltammetry, chronoamperometry, and chronopotentiometry and derivatives of these techniques.  
  • Pulse Voltammetry - Techniques such as pulse voltammetry, square wave voltammetry, and associated stripping techniques such as anodic stripping voltammetry.  
  • DC Corrosion - Run standard DC corrosion tests such as polarization resistance, potentiodynamic, cyclic polarization, and galvanic corrosion in addition to a number of others.
  • Electrochemical Energy - Test single-cells and stacks of various batteries, fuel cells or supercapacitors. Includes charge, discharge, cyclic charge-discharge techniques, potentiostatic, galvanostatic, self-discharge, leakage rate, and read cell voltage.
  • Electrochemical Signal Analyzer -  Designed specifically for the acquisition and analysis of time-dependent electrochemical noise signals. Cell voltage and current are continuously monitored at rates from 0.1 Hz to 1 kHz. A full featured set of analysis tools provides powerful analysis features such as statistical analysis, detrending, impedance spectra, and histogram analysis.
  • Electrochemical Frequency Modulation - A non-destructive corrosion rate measurement technique. It allows for measurement of the corrosion rate without prior knowledge of the Tafel constants. In addition, the technique determines the Tafel constants and provides 2 internal validity checks.
  • Critical Pitting Temperature - controls a Gamry Potentiostat, TDC4 Temperature Controller, and associated accessories to automatically measure the Critical Pitting Temperature of a material.
  • Electrochemical Noise - A more general form of electrochemical noise testing. It is also an ECM8 Multiplexer compatible electrochemical noise software package. 
  • Electrochemical Impedance Spectroscopy - includes experimental scripts for potentiostatic, galvanostatic and hybrid impedance spectroscopy experiments in addition to single frequency techniques like Mott-Schottky. We also have our unique power-leveling multisine technique that improves signal-to-noise across the spectrum. On the analysis side, it provides tools for fitting spectra to equivalent circuit models, Kramers-Kronig transform for data validation and a graphical model editor. Our software even includes a script for EIS simulation.
  • eChemAC - Includes full capabilities of eChemDC Toolkit plus allows electrochemical impedance spectroscopy (EIS) and EFM experiments.

 

Other options

  • 2, 3, and 4 electrode measurements
  • Electrical Isolation
    • Floating instrument: use with autoclaves, mechanical stress apparatus, or pipeline probes.
  • Portable
    • Size of a chemistry textbook, weighing only 3 kgs (6.6 lbs). Easy USB 2.0 connection to a Windows computer.
  • Built-In EIS
    • On-board DDS to perform EIS from 10 µHz to 1 MHz. 
  • DSP (Digital Signal Processing) Mode
    • Oversamples for improved signal-to-noise and accurate capacitance measurements.
  • Current Interrupt and Positive Feedback iR Compensation
    • Gamry potentiostats and their controlling software use control loop algorithms to accurately measure and correct for uncompensated resistance.
  • Auxiliary I/O
    • Control additional equipment via additional I/O interfaces: external signal input, analog voltage output, analog current output, auxiliary A/D input, and digital I/O connector.
  • Warranty
    • Protected by 2-year factory service warranty.

 

Specs and Images

 

 
REFERENCE 600
Potentiostat YES
Galvanostat YES
Zero Resistance Ammeter YES
Cell Connections 2, 3, or 4
Floating (Isolated from Earth)  YES
   

WEIGHT

3 kg

DIMENSIONS

9 (W) x 19 (H) x 27 (D) cm
   

SYSTEM

 
Max Current ± 600 mA
Current Ranges 11 (60 pA - 600 mA)
Current Ranges (w/Internal
Gain applied)
13 (600 fA - 600 mA)
Min Voltage Resolution 1 μV
Min Current Resolution 20 aA
Max Applied Potential ± 11 V
Rise Time <250 ns
Noise and Ripple <10 μV rms
Noise and Ripple (typical) <2 μV rms
Min Time Base 3.333 μs
Max Time Base 715 s
Min Potential Step 12.5 μV
   

EIS MEASUREMENT

 
Frequency Range 10 μHz - 1 MHz
EIS Accuracy See Accuracy
Contour Plot
Max AC Amplitude

3 V max
600 mA max

   

CONTROL AMP

 
Compliance Voltage ± 22 V
Output Current > ± 600 mA
Speed Settings 5
Unity Gain Bandwidth  980, 260, 40, 4, 0.4 kHz
   

ELECTROMETER

 
Input Impedance >1014 Ω
Input Current <5 pA
Input Current (typical) <2 pA
Bandwidth (-3dB) (typical) >15 MHz
Common Mode Rejection Ratio >80 dB (3 Hz)
>60 dB (1 MHz)
   

APPLIED POTENTIAL

 
Accuracy ± 1 mV ± 0.2% of setting
Accuracy (typical) ± 375 μV ± 0.04% of reading
Resolution 12.5 μV, 50 μV, 200 μV/bit
Drift <20 μV/°C
Potential Scan Range ± 0.4 V, ± 1.6 V, ± 6.4 V
   

MEASURED POTENTIAL

 
Accuracy ± 1 mV ± 0.2% of reading
Accuracy (typical) ± 250 μV ± 0.05% of reading
Full-Scale Ranges 12 V, 3 V, 300 mV, 30 mV
Resolution 400 μV, 100 μV, 10 μV, 1 μV/bit
Offset Range ± 10 V
   

CURRENT

 
Applied/Measured Accuracy ± 10 pA ± 0.05% of range 
± 0.2% of value (600 mA-6 nA)
or 0.75% of value (600 pA)
or 1.5% of value (60 pA)
Applied/Measured Resolution 0.0033% full-scale/bit
Bandwidth (-3 dB)
NOTE: Bandwidth is current 
         range dependent.
> 10 MHz (600 mA - 600 μA)
> 1.5 MHz (60 μA)
> 0.15 MHz (6 μA)
Stability Settings 4
Post Offset Gain 1, 10, 100
Offset Range ± 1X full-scale
   

iR COMPENSATION

 
Mode Current Interrupt and
Positive Feedback
Min Interrupt Time 33 μs
Max Interrupt Time 715 s
   

AUXILIARY A/D INPUT

 
Range ± 3 V
Resolution 0.1 mV
Input Impedance >100 kΩ or >10 GΩ
   

AUXILIARY D/A OUTPUT

 
Range 0-4 V
Resolution 1 mV